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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-25
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filingDate 1987-09-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_af84559256592231d3274832e2972556
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publicationDate 1989-03-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S6463566-A
titleOfInvention Production of n-substituted aminoethanethiol
abstract PURPOSE:To enable economical production of the title compound by forming N-substituted 2,2-dialkylthiazolidine from a reagent corresponding to the subject compound and 2,2-dialkylthiazolidine and hydrolyzing the product in the presence of hydrohalogenic acid. CONSTITUTION:The reaction of a compound of formula R<1>-Y (R<1> is 1-20C alkyl; Y is COX, N=C=O, CH2X; X is halogen) with another compound of formula I (R<2>, R<3> are methyl, ethyl) is carried out, preferably at an equimolar ratio in the absence or presence of a solvent at 0 deg.C up to the boiling point of the solvent to give a compound of formula II (Z is CO, NHCO, CH2). Then, the product is hydrolyzed in the presence of a hydrohalogenic acid such as hydrochloric acid or hydrobromic acid under relatively mild conditions at 0 deg.C to the refluxing temperature to give the subject compound of formula III which is used as an intermediate of medicines, photographic reagents or cosmetics.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-5002908-A
priorityDate 1987-09-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 30.