http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S6416747-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_33dafb5bbc2ec47ebcb7becbbe60f704 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B57-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C61-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C51-487 |
filingDate | 1987-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_41f2aebd233ca56fc5383c3afc4c294c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aa9adfb6c7c1ca68c4c82ee0193ef047 |
publicationDate | 1989-01-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-S6416747-A |
titleOfInvention | Method for optically resolving (+-)-cis-permethric acid |
abstract | PURPOSE:To resolve (+ or -)-cis-permethric acid and (-)-cis-permethric acid in good yield and high purity, by treating (+ or -)-cis-permethric acid using a specific optical resolution agent. CONSTITUTION:An optically active 1-(p-tolyl)ethylamine or optically active cis-N-benzyl-2-(hydroxymethyl)cyclohexylamine is added to (+ or -)-cis-permethric acid and the mixture is dissolved in a solvent such as methanol while heating and cooled to give supersaturation and a diastereoisomer is deposited. Then the diastereoisomer is treated with a base and further reacted with an acid to provided the aimed product. The above-mentioned optical resolution agent is used at an amount of 0.8-1 equivalent based on the (+ or -)-cis-permethric acid. |
priorityDate | 1987-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 30.