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filingDate 1987-05-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_01d0fc0e5e05bc51fa7dc3d199b54a77
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publicationDate 1988-12-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S63295408-A
titleOfInvention Method for purifying aqueous hydrazine hydrate solution
abstract PURPOSE: To obtain the titled high quality soln. having a remarkably lowered concn. of TOC (total org. carbon) by distilling an aq. hydrazine hydrate soln. in the presence of a salt of an inorg. acid or the like to distill off TOC and by distilling the resulting concd. soln. again. n CONSTITUTION: NH 3 is oxidized with an oxidizing agent such as H 2 O 2 in the presence of ketone and the resulting ketazine is hydrolyzed and purified by distillation to obtain an aq. hydrazine hydrate soln. 1 having about 500W1,500ppm TOC (total org. carbon) content. The soln 1 is fed to the lower part of a distilling column A, a soln. 2 of hydrochloride, sulfate, phosphate, carbonate or the like of hydrazine such as neutral hydrazine sulfate is fed to the upper part of th column A, thus to concentrate the soln. 1 by distillation. Water 3 contg. TOC is discharged from the top of the column A and the concd. soln. is drawn out of the bottom of the column A, fed to a distilling column B and distilled again. A purified hydrazine hydrate soln. 4 is recovered from the top of the column B. n COPYRIGHT: (C)1988,JPO&Japio
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type http://data.epo.org/linked-data/def/patent/Publication

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