http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S63211280-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_8e43b4ca6b41ce9f54c9a895d474c81a |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D417-04 |
filingDate | 1987-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_655df5e23283ac83632e8044df3adba0 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0cb4d1db6c3d7e1f5562e9e0e8e31777 |
publicationDate | 1988-09-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-S63211280-A |
titleOfInvention | Production of 2-(4-thiazolyl)benzimidazole |
abstract | PURPOSE: To obtain the titled high-purity compound useful as a mildew-proofing agent and a vermicide for animals by one-stage reaction, readily and in high yield, by reacting 4-thiazolecarboxylic acid with o-phenylenediamine as raw materials in an organic solvent under heating. n CONSTITUTION: 1mol. 4-thiozolecarboxylic acid is reacted with 0.9W2mol. o- phenylenediamine in an organic solvent optionally 0.01W0.1mol. acid such as boric acid as a catalyst at preferably ≥90°C, especially preferably 120W200°C for 3W30hr and a given amount of water is distilled away to give the aimed compound without using expensive reagent. o-Dichlorobenzene, phenyl ethyl ether, toluene, p-nitrotoluene or diglyme may be cited as the organic solvent and the amount of the organic solvent used is 3W30 times as much as that of 4-thiazolecarboxylic acid. n COPYRIGHT: (C)1988,JPO&Japio |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-102363616-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-9425458-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113289691-A |
priorityDate | 1987-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 44.