http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S63154767-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_8e43b4ca6b41ce9f54c9a895d474c81a |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B47-06 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B47-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B47-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B47-00 |
filingDate | 1986-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ae01bf2e00ef0bd2d1bb65a660b01a8a |
publicationDate | 1988-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-S63154767-A |
titleOfInvention | Preparation of naphthalocyanines |
abstract | PURPOSE: To prepare naphthalocyanines in a high yield and a high purity under mild conditions, by reacting 2,3-naphthalenedicarboxylic acid (anhydride) with a metal (compound) and urea in the presence of a catalyst in a specified solvent. n CONSTITUTION: 2,3-Naphthalenedicarboxylic acid of formula I (where X is H, a halogen or an alkyl, aryl, alkoxy, nitro or carboxyl group; and m is 1W6) and/or 2,3-naphthalenedicarboxylic anhydride of formula II (where X and m are the same as above) is reacted with a metal and/or a compound thereof (e.g. anhydrous aluminum chloride) and urea in the presence of a catalyst (e.g. ammonium molybdate) in 1,3-dimethyl-2-imidazolidinone as a solvent to give naphthalocyanines of formula III (where and m are the same as above; M is a metal, a metal oxide or a metal halide). The use of the above-mentioned catalyst makes it possible to produce the title compound in a high yield and a high purity under mild conditions, without requiring high temperatures unlike the conventional methods. n COPYRIGHT: (C)1988,JPO&Japio |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110724150-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-110724150-B |
priorityDate | 1986-12-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 33.