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filingDate 1984-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3e547371754d0ab23c3cfbf19a4bf528
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publicationDate 1986-03-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S6156161-A
titleOfInvention Preparation of 2-methyl-3-pyrazolidone
abstract PURPOSE: To obtain the titled compound useful as a synthetic intermediate of penicillin, antiobesity agent, anti-enzymatic agent, etc., easily, in high yield, from an inexpensive raw material, by the hydrolytic cyclization of N-methyl, N'-β-cyanoethyl-hydrazine. n CONSTITUTION: The objective compound of formula II can be prepared by the hydrolytic cyclization of novel N-methyl, N'-β-cyanoethyl-hydrazine of formula I in the presence of water, using a mineral acid, preferably hydrochloric acid, sulfuric acid, nitric acid, etc., at the refluxing temperature of water. The starting compound of formula I can be produced by the hydrogenation of formaldehyde β-cyanoethylhydrazone, 1,4-di(β-cyanoethyl)hexahydro-1,2,4,5-tetrazine or their mixture. n COPYRIGHT: (C)1986,JPO&Japio
priorityDate 1984-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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