http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S61266955-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_02ff914937eb6ceaee5ca69cc56cbfa7 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09K19-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J20-281 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J20-292 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N30-88 |
filingDate | 1985-05-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_96c65209ae46eff5356fb6eb3eea2aa5 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7e846db192f60806db177ae7d608a66a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bcece100bfe464983e3165c29da9905f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bee9a86a7054ec2acf8c8a4376c4d4c0 |
publicationDate | 1986-11-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-S61266955-A |
titleOfInvention | Liquid crystal material for stationary liquid phase of gas chromatographic analysis |
abstract | PURPOSE: To obtain a liquid crystal material for a stationary liquid phase for gas chromatographic analysis which can be used over a wide temp. region by using 2-chloro-N,N'-bis-(4-butoxybenzylidene)-phenylene-1,4-diamine. n CONSTITUTION: Explanation is made with an embodiment. The sulfate (5g) of 2-chloro-phenylene 1,4-diamine is dissolved in an ethanol solvent (200ml) contg. triethyl amine (4.6g) as a strong basic material and slightly excessive 4-butoxylbenzaldehyde (8.9g) is added thereto. Such soln. mixture is subjected to heating reflux for about 15hr. The intended liquid crystal material (8.0g) is settled and formed when the soln. is thereafter allowed to cool. The material is refined by the recrystallization using a suitable solvent such as ethanol. Such liquid crystal material exhibits only the nematic liquid crystal phase over a wide temp. range from about the room temp. to 230°C and therefore the quick and simple sepn. of various org. mixtures is made possible if such material is utilized for the stationary liquid phase of the gas chromatograph. n COPYRIGHT: (C)1986,JPO&Japio |
priorityDate | 1985-05-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 29.