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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C409-12
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C407-00
filingDate 1985-02-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_84a0e11030a49320ff9208a0d9e5f55c
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_24f959ce926505e829bbfe9dab395538
publicationDate 1986-08-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S61180764-A
titleOfInvention Oxidization of p-diisopropylbenzene
abstract PURPOSE: To obtain p-diisopropylbenzene dihydroperoxide, smoothly in high yield, by the liquid-phase oxidization of p-diisopropylbenzene with molecular oxygen at a specific reaction temperature. n CONSTITUTION: p-Diisopropylbenzene (abbreviated as p-DIPB) is oxidized with molecular oxygen in the presence of an alkaline aqueous solution at <100°C, and the oxidization is continued thereafter by combining the step to raise the temperature and the step to keep the reaction temperature at a constant level. The reaction temperature is maintained to <100°C until the conversion of p- DIPB reaches 70%, and raised to 103W110°C when the conversion reaches 70W90%. The objective compound can be produced by continuing the oxidation reaction until the hydroperoxide concentration in the oxidization product reaches ≥20wt% in terms of p-diisopropylbenzene monohydroperoxide and reaches to a level higher than the hydroperoxide concentration before heating to 103W110°C by ≥10wt%. n COPYRIGHT: (C)1986,JPO&Japio
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priorityDate 1985-02-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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