http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S6016956-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_6cfc033f059d282fcd915bc8be2ae53f |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-52 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C221-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C213-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07B61-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C225-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J23-44 |
filingDate | 1983-07-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1ef00d60ccbd122266334c8968452718 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_07acd45dd1c4cc155e030a761f04a8b7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aad937183d2ecc9440ae4151d036a911 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_52e976728f45b457e3ae669fbc44025f http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3a2257ce3a552cca415e968d2ddd41f3 |
publicationDate | 1985-01-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-S6016956-A |
titleOfInvention | Production of 3,3' -or 3,4'-diaminobenzophenone |
abstract | PURPOSE: To produce the titled compound useful as a raw material of agricultural chemicals and pharmaceuticals, an intermediate of dyes, etc., in high yield, by reducing a benzophenone compound with formic acid or a formic acid salt in the presence of palladium catalyst, and dechlorinating the reduction product. n CONSTITUTION: The objective 3,3'- or 3,4'-diaminobenzophenone is produced by reducing the benzophenone compound of formula (X is Cl substituted to 4 or 6 position; Y is H or Cl, when Y is H, the position of the amino group is 3' or 4', and when Y is 4'-Cl, the amino group is 3') with formic acid or a formic acid salt in the presence of a palladium catalyst (e.g. palladium activated carbon), and dechlorinating the reaction product. The amount of the catalyst is 0.01W10wt% based on the benzophenone compound used as the raw material. The formic acid or the formic acid salt is used in the form of an aqueous solution, and its amount is slight excess to the stoichiometric amount. The solvent is usually the one miscible with water, e.g. alcohol. The reaction is carried out usually at 30W110°C. n COPYRIGHT: (C)1985,JPO&Japio |
priorityDate | 1983-07-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.