http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S60130565-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_be92719b856db86c092cc233e9512ca2 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-20 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B41M5-155 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C313-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00 |
filingDate | 1983-12-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e76960ac9495d51bae1107d16bd3f8f1 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_df7abc07020eba277ac259512d970fd4 |
publicationDate | 1985-07-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-S60130565-A |
titleOfInvention | Production of 1,7-di(4-hydroxyphenylthio)-3,5-dioxaheptane |
abstract | PURPOSE: To produce the titled compound useful as a color developer of leuco dyes, with simple operation, in high yield and purity, by hydrolyzing 4-thiocyanophenol under alkaline condition, and reacting with bis(2-haloethoxy)methane. n CONSTITUTION: 4-Thiocyanophenol is hydrolyzed in the presence of excess alkali (e.g. NaOH, KOH, etc.) to obtain 4-mercaptophenol. The objective compound is produced by adding bis(2-haloethoxy)methane to the reaction mixture, and reacting preferably in the presence of a phase transfer catalyst (e.g. a quaternary ammonium salt) at 15W40°C. The amount of bis(2-haloethoxy)methane is 0.5mol per 1mol of 4-mercaptophenol, and the reaction of the mixture is carried out by using 0.1mol of the catalyst. n COPYRIGHT: (C)1985,JPO&Japio |
priorityDate | 1983-12-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 29.