http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S60115554-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_3afd226eda66c2a4d1ca587afc0c5edd |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C217-20 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C213-00 |
| filingDate | 1983-11-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7b1e1cbe231459dd9055252b68262513 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_374603300d8a891cca37108e3db45725 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8c457d9ceaa29411a2ca2abb83afd534 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8ae8760a0a88e4495d0180ca0aea6e00 |
| publicationDate | 1985-06-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | JP-S60115554-A |
| titleOfInvention | Production of deacetylmoxisylyte |
| abstract | PURPOSE: To obtain the titled compound useful as a synthetic intermediate for sympatholytic agents and medicines for cardiovascular organs in high purity and yield, by hydrolyzing the acetyl group in an N,N-dimethylethylamine derivative, diazotizing the hydrolysis product, and distilling the diazotization product under reduced pressure. n CONSTITUTION: The acetyl group in 2-(4-acetamino-2-isopropyl-5-methylphenoxy)- N.N-dimethylethylamine of formula I is hydrolyzed with an aqueous solution of hydrochloric acid or sulfuric acid, etc. and then diazotized with a nitrite, e.g. sodium nitrite. In the final stage, the diazotization product is then heated at ≤180°C under ≤1mmHg reduced pressure to afford the aimed substance 2-(4-hydroxy-2-isopropyl-5-methylphenoxy)-N,N-dimethylamine (DAM) of formula II. n COPYRIGHT: (C)1985,JPO&Japio |
| isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109134281-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109134281-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0728479-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0694300-A1 |
| priorityDate | 1983-11-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 34.