http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S5781499-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P9-12
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K36-896
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07J9-00
filingDate 1980-11-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ab9c684cbd85cbefa163195ee4b6aa79
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f8c38a7f236261229af789c40990915a
publicationDate 1982-05-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S5781499-A
titleOfInvention Production of ecdysone
abstract PURPOSE: Bodies of Paris verticillata M.v. Bieb are extracted to obtain ecdysones used as an insect metamorphosis hormon in high yield with industrial advantage. n CONSTITUTION: For example, Paris verticillata, M.v. Bieb is extracted with a solvent such as methanol and the extract is concentrated to give the primary extract. Then, the extract is extracted with a solvent of butanol-water system and the organic layer of the extract is concentrated under reduced pressure to give the secondary extract. The product is subjected to column chromatography and the eluate is acetylated. The product is subjected to column chromatography again and the eluate is hydrolyzed to give ecdysone of formula I. The eluate of the secondary extract is treated with Sephadex LH-20 and eluted to give a flavonol derivative of formula II (R is H, -D-glucose), a new compound, used as a hypotensor. n COPYRIGHT: (C)1982,JPO&Japio
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2011046645-A
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