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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C229-42
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filingDate 1980-10-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b4a55fc21c7edb9036016999082bde4b
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2c415f77e7fcab86c7c861d30c6f79a7
publicationDate 1982-05-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S5775954-A
titleOfInvention Preparation of 2-(2,6-dichlorophenyl)amino-phenylacetic acid or its salt
abstract PURPOSE: To obtain the titled compound in high yield advantageously, by reacting a dichloroaniline derivative with a methylthioacetic acid or its derivative, followed by reaction with a halogenating agent and a Lewis acid, alkali hydrolysis and reductive desulfurization reaction. n CONSTITUTION: N-Phenyl-2,6-dichloroaniline is reacted with methylthioacetic acid or its reactive derivative at its carboxyl group, to give N-phenyl-N-methylthioacetyl-2,6-dichloroaniline. This compound is reacted with a halogenating agent (e.g., α-chlorosuccinimide, Cl, etc.) and a Lewis acid to give 1-(2,6-dichlorophenyl)-2- oxo-3-methyl-thioindoline. This compound is subjected to alkali hydrolysis and reductive desulfurization reaction successively or in the reverse order to give the desired compound. n EFFECT: The reaction process is short, the reaction conditions are mild, and environmental pollution problems will not take place. n COPYRIGHT: (C)1982,JPO&Japio
priorityDate 1980-10-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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