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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C51-34
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filingDate 1980-10-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_96555f7fcccebf32e13af77c8ee2e254
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_48df4b896e540aeda556351927b1d220
publicationDate 1982-04-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S5764637-A
titleOfInvention Production of dodecanedioic acid
abstract PURPOSE: Cyclododecane, cyclododecanol or cyclododecanone is dissolved in halogenated hydrocarbon, acetic acid or aqueous acetic acid and the ozone oxidation is conducted in a water-repellent reactor at low temperature to produce the titled substance in high yield. n CONSTITUTION: At least one of cyclododecane, cyclododecanol or cyclododecanone is dissolved in a halogenated hydrocarbon or an aqueous acetic acid of more than 70%(v/v) concentration, or acetic acid and the one-stage oxidation is conducted in a water-repellent reactor with an ozone-containing gas at 30W100°C to produce the reaction mixture mainly consisting of dodecanedioic acid. the reactor can get water-repellent by the treatment with a polymerizable silicon compound such as dichlorodimethylsilane or lining with a water-repellent resin such as a silicone resin, fluororesin or polyethylene resin. n EFFECT: As the rector is water-repellent, the product does not stick to the reactor. The consideration on the reaction waste is in no need. n COPYRIGHT: (C)1982,JPO&Japio
priorityDate 1980-10-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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