http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S5742656-A

Outgoing Links

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C69-36
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-36
filingDate 1980-08-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_149aed038b16ed62f0b327d9b7b07241
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publicationDate 1982-03-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S5742656-A
titleOfInvention Continuous preparation of oxalic acid diester
abstract PURPOSE: To obtain the titled compound continuously useful as a raw material for synthesizing oxalic acid, etc., by subjecting the reaction product of CO and an ester of nitrous acid to separating process through condensation, reprocessing process of a noncondensing gas, distillation process of a condensate, and hydrolyzing process of by-product. n CONSTITUTION: A gas comprising CO, an ester of nitrous acid, etc. is sent through the pipe 21 to the reactor 1 filled with a catalyst and reacted. The reaction product gas is sent to the condenser 2 and cooled, the condensate is sent through the pipe 14 to the distillation column 4. A noncondensing gas is sent through the pipe 12 to the reprocessing column 3, and the gas is brought into contact with a molecular oxygen- containing gas and an alcohol so that NO in the gas is processed to reproduce the ester of nitrous acid, which is sent through the pipes 19 and 21 to the reaction process. A carbonic acid diester, etc. is distilled by the distillation column 4, and an oxalic acid diester is taken out from the pipe 22. The distillate is sent through the pipes 23W25 to the hydrolyzing column 5 and hydrolyzed to give an alcohol, which is sent through the pipes 26, 28, and 18 to the reprocessing column 3. n COPYRIGHT: (C)1982,JPO&Japio
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2014129283-A
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priorityDate 1980-08-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

Incoming Links

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Total number of triples: 24.