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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D231-20
filingDate 1980-05-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_57a0e83a6670cc03b6f626c4dfcd174a
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publicationDate 1982-01-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S572275-A
titleOfInvention Preparation of 4-benzoylpyrazole-type compound
abstract PURPOSE: To prepare the titled substance from an inexpensive raw material, in a short time, easily, in high yiekd, by reacting a benzotrichloride-type compound, a benzoic acid-type compound, and a pyrazolone-type compound in the presence of a catalyst. n CONSTITUTION: A compound of formula I (X and Y are H or halogen), a compound of formula II and a compound of formula III (R is lower alkyl) are made to react together in the presence of a catalyst to obtain a compound of formula IV (Z is H or metal atom). The catalyst is a metal halide or an acid such as sulfuric acid, phosphoric acid, perchloric acid, etc., especially pref. magnesium chloride or zinc chloride. The reaction is carried out if necessary in a solvent. The solvent is pref. the one having a bailing point of ≥130°C, e.g. nitrobenzene, dichrlorobenzene, etc. The amount of the compound of formula I is equimolar amount of the compound of formula II, and that of the compound of formula III is 1mol/mol of the sum of the compounds of formula I and II. n COPYRIGHT: (C)1982,JPO&Japio
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priorityDate 1980-05-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 35.