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filingDate 1980-03-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6dd2f2e0d3da9dec8f7cfe465858b67a
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publicationDate 1981-10-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S56128730-A
titleOfInvention Preparation of trimellitic acid
abstract PURPOSE: To obtain the titled compound in high yield, by the air oxidation of pseudocumene in the liquid phase in the batchwise reaction according to the specified absorption of oxygen at a relatively low temperature in the first stage, and in the continuous completely mixing reaction at higher temperatures in the second stage. n CONSTITUTION: One mole of of pseudocumene is oxidized with air in the liquid phase, by the batchwise reaction in the oxygen absorption of 2.8mol or more at 110W170°C in the first stage and by the continuous completely mixing reaction at 180W240°C, more preferably at 195W225°C in the second stage, in the presence of cobalt, manganese and bromine as a catalyst, in acetic acid, to give trimellitic acid. n EFFECT: The final yield is increased to 80W88%, the catalyst may be readily recoverable. Furthermore, the oxidation stage at a high temperature can be carried out safely. n USE: High grade plasticizer or a raw material for heat-resistant plastics. n COPYRIGHT: (C)1981,JPO&Japio
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