http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S5559134-A

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filingDate 1978-10-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9f2aac163a5210e7c8c51c848bcbbde2
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publicationDate 1980-05-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S5559134-A
titleOfInvention Improved method of making naphthalic acid or its anhydride
abstract PURPOSE: An acenaphthene is oxidized by a two-step process in which the second oxidation is conducted in a mixture of an aqueous alkali and an organic solvent to produce said naphthalic acid or its anhydride useful as intermediate of dyes and pigments in high yield and purity. n CONSTITUTION: Acenaphthene or an acenaphthene derivative sustituted with proups other than hydroxyl and amino groups is oxidized with a molecular oxygen- containing gas or nitric acid and the resulting product is further oxidized with a hypohalous salt or a molecular oxygen-containing gas, wherein the second step oxidation is conducted in a mixture of sufficient amount of an aqueous alkali to dissolve the stoichiometric amount of naphthalic acid and 0.1W800, preferably 1W 80vol% of an organic solvent to improve greatly the efficiency of the second step oxidation, thus giving high-purity naphthalic acid or its anhydride in high yield for a short reaction time. n COPYRIGHT: (C)1980,JPO&Japio
priorityDate 1978-10-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 30.