http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-S55167264-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_24aca9ded2638ea793d05360dde7a4a0 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-43 |
filingDate | 1979-06-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7e41061a52a178a49cbba614ac8675dc http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_565b6e5283e5687a9310afbe0c066a21 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5f6c832adb42a6c120ad07f1763ff9ac http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_42e3836f0a029ad3910b7bfbc9ba5d90 |
publicationDate | 1980-12-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-S55167264-A |
titleOfInvention | Preparation of 2-amino-4-acylaminophenyl ether |
abstract | PURPOSE: To obtain the titled compound useful as an intermediate for an azo disperse dye in high selectivity and high yield, by maintaining the pH of the reaction mixture of a 2,4-diaminophenyl ether with an acylating agent in water and an organic solvent at a specific value. n CONSTITUTION: A 2,4-diaminophenyl ether, e.g. a compound of formula I (R is alkyl or phenyl group), is acylated with an acylating agent in water and an organic solvent at a pH of 6W10, preferably 6W8, by adding a base thereto, at a low temperature, preferably 0W20°C, to give a 2-amino-4-acylaminophenyl ether of formula II (A is acyl group). A by-product 2-acylamino derivative is scarcely formed with the amount of a by-product 2,4-bis(acylamino)derivative of 5% or less. n COPYRIGHT: (C)1980,JPO&Japio |
priorityDate | 1979-06-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 26.