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filingDate 1977-12-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a2824e25e1a515e86d7daa2991ad2c5d
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publicationDate 1979-06-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-S5479241-A
titleOfInvention Production of p-toluic amide
abstract PURPOSE: The reaction between methyl p-toluate and ammonia is conducted in the presence of an ammonium salt of strong acid as a catalyst at an adequate temperature to produce inexpensively title compound useful as an intermediate for dyes and pigments at high reaction rate in high yield. n CONSTITUTION: In the reaction between methyl p-toluate and an excess amount, preferably 1W10 times the molar quantity of p-toluate, of ammonia, 5W30 mole% of an amminium salt of strong acid with a pK of less than 1 as ammonium chloride or ammonium nitrate is used as a catalyst to yield p-toluic amide. The methyl p- toluate is prepared by esterifying p-toluic acid resulting from the oxidation of p- xylene with air with methanol. n EFFECT: Ammonium salts as catalysts are inexpensive and readily available in large amounts. n COPYRIGHT: (C)1979,JPO&Japio
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0355480-A2
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type http://data.epo.org/linked-data/def/patent/Publication

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