http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-H11269484-A

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filingDate 1999-01-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_054c711a5c5a128b61b56c81b658b82a
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4852510aaa685f18f7ee869f800fd5f8
publicationDate 1999-10-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H11269484-A
titleOfInvention Carboxylate overbased gel
abstract PROBLEM TO BE SOLVED: To provide a method for preparing an excellent overbased gel substance and a coating or other substance containing this substance. A method for preparing an overbased calcium carboxylate gel comprising the following steps. I) treating a carboxylic acid of about 8-30 C / reactive equivalents thereof in the presence of an organic solvent with an oxidation or an equivalent ratio of calcium hydroxide to carboxylic acid of about 2: 1 to 10: 1; II). Carbonating the mixture of I at about 50-100 ° C in the presence of an accelerator system comprising water and a C1-8 alcohol; wherein the alcohol / water molar ratio is substantially constant; The ratio of the mixture of I is such that the viscosity of the mixture is not more than about 1000 CP during the process, and in particular the amount of alcohol in the case of calcium hydroxide is adjusted throughout the process so as to maintain this viscosity; 25-11 Gelling the mixture of II at 0 ° C .; wherein II and I No stripping during step II; IV) removing alcohol and water if necessary.
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