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classificationCPCAdditional http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-52
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-38
filingDate 1997-10-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e3ca4bf0ec2838801b18fae3cde96896
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6318e9b40841c06172e325c34ceb6f18
publicationDate 1999-05-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H11130728-A
titleOfInvention Method for producing mono-tertiary alkyl malonate
abstract PROBLEM TO BE SOLVED: To provide a method for producing a high-purity mono-tertiary-malonic acid alkyl ester by a simple method using inexpensive malonic acid dimethyl ester or malonic acid diethyl ester as a raw material. SOLUTION: The method for producing a mono-tertiary-alkyl malonic acid ester includes the following five steps (1) to (5). (1) A step of transesterifying malonic acid dimethyl ester or malonic acid diethyl ester with a tertiary alkyl alcohol in the presence of a catalyst. (2) a step of hydrolyzing the ester mixture obtained in the step (1) with an aqueous alkali solution. (3) a step of extracting and removing ditertiary alkyl malonate from the alkali hydrolysis-treated product obtained in step (2) using an organic solvent. (4) a step of acid-precipitating the aqueous phase obtained in the step (3). (5) A step of extracting malonic acid mono-tertiary alkyl ester from the acid precipitate obtained in step (4) using an organic solvent.
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http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-109354572-A
priorityDate 1997-10-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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