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inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0ad154f8f556ac1cbe5e02f3ccffb9ca
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publicationDate 1998-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H10195066-A
titleOfInvention Method for producing α-tocopherol or α-tocopheryl acetate
abstract PROBLEM TO BE SOLVED: To react 2,3,5-trimethylhydroquinone with phytol or isophytol in the presence of a zinc halide condensation catalyst and a proton donor, and then to or without esterification with acetic anhydride. By α -To provide a method for producing tocopherol or α-tocopheryl acetate. [MEANS FOR SOLVING PROBLEMS] The reaction is carried out in a non-polar solvent which is only slightly miscible with water and B. The required zinc halide is introduced into the reaction in the form of a mixture with 1 to 4 moles of water per mole of the same. The recycling of zinc halides is possible, in which case the yield and purity of α-tocopherol are not reduced.
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