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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B67-00
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filingDate 1996-12-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6ca65b7eddaa0f6a3d30b0ae93c7ffde
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publicationDate 1998-07-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H10183005-A
titleOfInvention Water-insoluble pyridone disazo dye and method for producing the same
abstract (57) [Problem] To provide an orange pyridone disazo dye capable of performing good dyeing under severe conditions at high temperature. SOLUTION: The diffraction angle (2θ) is about 6.9 °, about 15.4. The following has a crystalline modification characterized by X-ray diffraction (CuKα) showing strong peaks at ゜, about 18.8 ° and about 25.7 °, and also intermediate peaks at about 12.2 ° and about 26.7 °. A water-insoluble pyridone disazo dye represented by the structural formula (I), 4 ′-(4-hydroxyphenylazo) aniline and 6-hydroxy-1,4-dimethyl-2 -The coupling reaction product with oxo-1,2-dihydro-3-pyridinecarbonitrile was converted to 2,4-difluoro- The cake obtained by subjecting 6- (di-n-butylamino) 1,3,5-triazine to a condensation reaction in acetone is treated under specific conditions to form a β-type crystal modification or to carry out the condensation reaction with N, A method for producing the pyridone-based disazo dye, which comprises conducting the reaction in N-dimethylformamide and releasing the condensation reaction product into water to precipitate crystals of β-form modification. Embedded image
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9359503-B2
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