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filingDate 1994-08-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a670a5832fa49f6763e02f3e42068c09
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publicationDate 1996-02-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H0853392-A
titleOfInvention Method for producing 4-hydroxybutyl (meth) acrylate
abstract (57) [Summary] [Objective] To obtain 4-hydroxybutyl (meth) acrylate of suitable quality as a monomer for polymerization without going through a distillation step. [Structure] A reaction mixture of 1,4-butanediol and (meth) acrylic acid is subjected to liquid-liquid extraction with a water-insoluble organic solvent and water to obtain an aqueous phase containing 4-hydroxybutyl methacrylate. Is treated with activated carbon and then extracted with a polar organic solvent to transfer 4-hydroxybutyl methacrylate to the organic solvent phase. The organic solvent is distilled off from this organic solvent phase to obtain 4-hydroxybutyl methacrylate. [Effect] A high quality product can be obtained by a simple operation of activated carbon treatment.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2007106749-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-4506237-B2
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2005281274-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2007161636-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2009530425-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-100787056-B1
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2012529454-A
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