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filingDate 1996-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f47a0a449aa374dc745266372300403d
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publicationDate 1996-10-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H08283215-A
titleOfInvention Fractionation and purification of aromatic polyamine mixture and its use
abstract (57) [Abstract] (Corrected) [PROBLEMS] To provide a method for facilitating the fractional distillation and purification of a diphenylmethane-based aromatic polyamine mixture and obtaining an isomer in a highly pure state or a concentrated state. . A) a starting polyamine mixture in a first extraction step (i) a hydrophobic solvent and optionally an aromatic auxiliary amine) and optionally a hydrophobic solvent phase consisting essentially of polyamine, (ii) ) Mixing with a two-phase system consisting of an aqueous phase consisting of water, a strong acid and an auxiliary amine and optionally a polyamine, introduced into the first extraction stage and draining the aqueous phase and the first organic phase. b) fractionating the first organic phase in a first distillation stage, c) adding a base to neutralize the first aqueous phase, and the resulting mixture into a second aqueous phase and a second organic phase. D) the second organic phase is subjected to a second distillation step in which (i) a distillate consisting essentially of a hydrophobic solvent and an auxiliary amine and (ii) a distillation consisting essentially of a second polyamine fraction. Separate into a residue.
priorityDate 1995-04-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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