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filingDate 1995-03-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1996-10-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H08253879-A
titleOfInvention Low-angle grain boundary manifestation corrosion method for steel materials
abstract (57) [Abstract] [Purpose] The present invention has been impossible with the prior art (1). Clear and clear method of revealing small-angle grain boundaries with no bubbles or corrosion unevenness on the corroded surface, and (2) Large-angle grain boundaries and small-angle grain boundaries on one sample that cannot be obtained by conventional observation methods. It is to provide an observation method capable of simultaneous identification. [Structure] A steel material is polished, pre-corroded with 0.03 to 0.1N hydrochloric acid, washed with water, and 0.1 to 0.2N oxalic acid and 30 to 40% by weight of hydrogen peroxide. -Angled grain boundary appearance corrosion of steel materials by immersing hydrogen peroxide water containing 0.1 to 0.2 N sulfuric acid and methanol or ethanol instead of methanol in a mixed solution of the following volume% for 3 to 20 seconds Method. Oxalic acid: Hydrogen peroxide solution: Sulfuric acid: Methanol or ethanol = 45-55: 45-55: 7-18: 1 (volume% ratio)
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priorityDate 1995-03-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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