http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-H08183796-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_c999fee6428152a996011d506925c2d7 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07K1-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07K5-072 |
filingDate | 1994-12-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f8ecaa1117822e07de4b3a540dcac5c8 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_21d7ff1f7862d752d840bf55708ca68e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f5dad737453eab9bc9e02570092c1945 |
publicationDate | 1996-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-H08183796-A |
titleOfInvention | Process for producing α-L-aspartyl-D-amino acid-N- (S) -α-alkylbenzylamide |
abstract | (57) [Summary] (Modified) [Purpose] α-L-aspartyl-D-amino acid-N- A method for producing (S) -α-alkylbenzylamide is provided. [Structure] Strong acid addition salt of L-aspartic anhydride and D -Amino acid-N- (S) -α-alkylbenzylamide is condensed to give α-of the general formula 1 with good reaction selectivity and high yield. L-Aspartyl-D-amino acid-N- (S) -α-alkylbenzylamide is obtained. Further, the reaction solution was made alkaline, and the excess D-amino acid-N- (S) -α-alkylbenzylamide was extracted and removed in an organic solvent, and the aqueous layer was adjusted to pH 4.5 to 6.5 for crystallization. Α-as crystals L-Aspartyl-D-amino acid-N- (S) -α-alkylbenzylamide is obtained. (R 1 represents a C1-4 alkyl group, and R 2 represents a C1-3 alkyl group.) |
priorityDate | 1994-12-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 56.