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filingDate 1992-10-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1994-04-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H06115904-A
titleOfInvention Method for producing potassium periodate
abstract (57) [Summary] [Structure] In the method for producing potassium periodate by oxidizing potassium iodate with chlorine, potassium hydrogen iodate, potassium carbonate, potassium dihydrogen phosphate are previously added to an aqueous potassium iodate solution. , One or more of dipotassium hydrogen phosphate is added 0.2 to 2 mole times, and then potassium hydroxide or potassium carbonate is added 1 to 6 equivalent times, while chlorine is added at a temperature of 50 to 95 ° C and a pH of 7 to 10. A method for producing potassium periodate, which comprises oxidizing with. [Effect] pH adjustment during chlorine oxidation can be easily adjusted within a narrower range, and even under mild conditions such as 100 ° C or less, 97% potassium periodate can be added. It is possible to manufacture with the above high yield. Further, a general-purpose glass-lined reactor or the like can be sufficiently used.
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