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filingDate 1990-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a8f654c759b882de0c2f756462278234
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publicationDate 1992-02-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H0454187-A
titleOfInvention Production of fluoran compound
abstract PURPOSE: To obtain the subject compound useful as a color-developing dye in a color-developing recording without producing tarry by-product at a low-cost by reacting a benzoic acid derivative with a phenol derivative in concentrated sulfuric acid in the presence of phosphoric acid. n CONSTITUTION: The objective compound of formula III can be produced by reacting a benzoic acid derivative of formula I (X is lower alkyl or halogen; m is 1 or 2) with a phenol derivative of formula II [R is H or lower alkyl; Ar is (substituted) phenylene or naphthylene; R 1 and R 2 are H or lower alkyl; Y is H or substituted amino group of formula N(R 3 )R 4 ; R 3 is H or lower alkyl; R 4 is lower alkyl, phenyl or naphthyl] in concentrated sulfuric acid in the presence of phosphoric acid at 0-50°C. The phosphoric acid to be added to concentrated sulfuric acid is preferably orthophosphoric acid and its amount is 0.5-25 wt.% based on the sulfuric acid. n COPYRIGHT: (C)1992,JPO&Japio
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type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 30.