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filingDate 1990-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1992-07-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H04187682-A
titleOfInvention Purification of glycidyl acrylate or glycidyl methacrylate
abstract PURPOSE: To efficiently remove non-reacted epichlorohydrin and by-produced chlorine compounds without lowering the recovery rate of the purified products, by subjecting crude glycidyl (meth)acrylate to a stripping treatment under a specific condition and subsequently distilling the treated product. n CONSTITUTION: Crude glycidyl (meth)acrylate containing non-reacted epichlorohydrin and by-produced chlorine compounds is bubbled with mixed gases comprising oxygen gas and an inert gas (preferably nitrogen gas) in the presence of a quaternary ammonium salt (preferably tetraethyl ammonium chloride) to strip the epichlorohydrin and the by-produced chlorine compounds, followed by distilling the treated product to provide the objective purified product. The stripping treatment is preferably carried out under a reduced pressure of 2-50mmHg at a temperature which is lower than the boiling point of the solution containing the crude glycidyl (meth)acrylate, etc., and which is higher than the boiling point of the epichlorohydrin. n COPYRIGHT: (C)1992,JPO&Japio
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