http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-H03195777-A

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B11-28
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B67-48
filingDate 1989-12-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b3ba57a1c190822f5697df74ff7b0fc5
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7f542088d61546b9012511c101c20cb5
publicationDate 1991-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H03195777-A
titleOfInvention Crystal transformation of 3-dibutylamino-6-methyl-7-anilinofluoran
abstract PURPOSE: To easily obtain the title low-melting anilinofluoran by dissolving a high-melting dibutylaminomethylanilinofluoran crystal in an organic solvent consisting mainly of carbon tetrachloride followed by cooling to effect recrystallization. n CONSTITUTION: 3-Dibutylamino-6-methyl-7-anilinofluoran crystal with a high- melting point of 179-186°C, characterized by the X-ray diffraction pattern having peaks at diffraction angles 6.9°, 11.0°, 18.5° and 18.9° determined by the X-ray diffraction method using Cu-Kα beams is dissolved in an organic solvent consisting mainly of carbon tetrachloride followed by cooling to effect recrystallization, thus obtaining the objective low-melting 3-dibutylamino-6- methyl-7-anilinofluoran with a melting point of 148-152°C, characterized by the X-ray diffraction pattern having peaks at diffraction angles 6.9°, 11.6°, 12.0°, 17.8°, 21.1° and 21.5°. n COPYRIGHT: (C)1991,JPO&Japio
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0526856-A2
priorityDate 1989-12-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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