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filingDate 1988-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1b704e3366ea06c0db964e027c33f02e
publicationDate 1990-01-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H02662-A
titleOfInvention Monoazo pigment, its manufacture, and its application
abstract PURPOSE: To manufacture a specified monoazo pigment containing only a remarkably small amount of PCB by azo-coupling a specified azonium salt with CH- acidic coupling component H-K in an aqueous medium under a specified condition. n CONSTITUTION: When a dichloro- or trichlorobenzol diazonium salt is azo- coupled with a CH-acidic coupling component H-K formed of acetoacetic arylamide or naphthol series in an aqueous medium, they are coupled at a pH value smaller than pH7 and a temperature of 0-50°C with interruption of nitric acid ion under the presence of a coupling assistant or coupling accelerator to provide a monoazo pigment of the formula (K is the residue of a CH-acidic coupling component of acetoacetic aryl amide or naphthol, series; n is 2 or 3). When this pigment is dissolved in conc. sulfuric acid, PCB component is transferred to a non-polar organic solvent followed by analysis by a known method, this pigment contains biphenyl chloride having four or more Cl atoms is contained in an amount of 25μg at the maximum per g thereof. n COPYRIGHT: (C)1990,JPO
priorityDate 1987-12-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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