http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-H0262890-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_03d0f52bb4069f8a19d70dcfb697c67a
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C12Q1-34
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08B37-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H15-203
filingDate 1988-08-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_71a6b3c6ca4ea28277596b168d5160cc
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f2d5ec863263157aaf76157dcaf7d03d
publicationDate 1990-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H0262890-A
titleOfInvention Polyacetyloligosaccharide derivative
abstract NEW MATERIAL:A compound expressed by formula I (n is 0-9; Ac is formula II; R and R' are H, alkyl or phenyl). n USE: A precursor of substrates for measuring enzymic activity. n PREPARATION: A compound expressed by formula III, together with α,α- dimethoxytoluene, p-toluenesulfonic acid and dimethylformamide, is stirred at 50-60°C under reduced pressure for 4hr and then cooled to ambient temperature. Pyridine, acetic anhydride and dimethylaminiopyridine are added and the resultant mixture is allowed to stand for 20hr, extracted with ethyl acetate and purified by silica gel chromatography. Furthermore, the reaction mixture is dissolved in methanol and 10% palladium carbon is added to carry out reaction under normal pressure in a hydrogen atmosphere for 6hr. After filtration, recrystallization from ethanol is performed to afford the objective derivative. n COPYRIGHT: (C)1990,JPO&Japio
priorityDate 1988-08-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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