http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-H01308257-A

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-61
filingDate 1988-06-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f1e50965cdba5e94449399bde655ecb1
publicationDate 1989-12-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H01308257-A
titleOfInvention Distillation of chlorinated pyridine
abstract PURPOSE: To prevent a compound useful as a synthetic intermediate for drugs and agricultural chemicals while preventing tar formation, by reacting pyridine with chlorine in the presence of a diluent in a gas phase, neutralizing and further distilling by using water. n CONSTITUTION: Pyridine is reacted with chlorine in the presence of a diluent such as carbon tetrachloride or water in a gas phase. The prepared reaction solution is neutralized with an alkali (e.g. NaOH) and separated to give an organic layer containing chlorinated pyridine. Water is added to the organic layer, which is distilled to give 2-chloropyridine and/or 2,6-dichloropyridine. The amount of water is preferably ≥ equivalent weight based on pyridine existing in the system. n COPYRIGHT: (C)1989,JPO&Japio
priorityDate 1988-06-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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