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filingDate 1987-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_03663bd50f72fee105c8abe93d634fbb
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publicationDate 1989-06-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-H01157951-A
titleOfInvention Production of 1,1,3,3-tetramethylbutylhydroperoxide
abstract PURPOSE: To obtain the title compound having safe handling, containing no acetone peroxide, in a short time, in high purity economically and advantageously, by reacting neopentyl dimethylcarbinol with hydrogen peroxide in the presence of sulfuric acid. n CONSTITUTION: Neopentyl dimethylcarbinol (hereinafter abbreviated as DIBOH) or isobutylene containing ≥50wt.% neopentyl dimethylcarbinol is reacted with hydrogen peroxide in the presence of sulfuric acid to give 1,1,3,3- tetramethylbutylhydroperoxide. In the reaction, the amount of sulfuric acid used is 0.5W2mol based on 1mol DIB-OH, that of hydrogen peroxide is 1W3mol and concentration of sulfuric acid in the mixed solution of sulfuric acid-hydrogen peroxide is 38W45wt.%. The reaction temperature is preferably 0W30°C. n COPYRIGHT: (C)1989,JPO&Japio
priorityDate 1987-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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