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filingDate 2012-08-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2013-03-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2013-03-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-5167450-B1
titleOfInvention Method for producing vanadium electrolyte
abstract Provided is a method for producing a vanadium electrolyte solution capable of producing a vanadium electrolyte solution having a high concentration capable of suppressing generation of sludge as efficiently as necessary. A step of preparing a first electrolyzed solution containing 1.5 to 3.8 mol / L of one or both of tetravalent and trivalent vanadium ions, and a step not containing or substantially not containing vanadium ions. A step of preparing two electrolyzed solutions, and an electrolyzing step of simultaneously performing oxidation-reduction electrolysis of the first and second electrolyzed solutions to obtain an electrolytic solution containing pentavalent or divalent vanadium ions from the first electrolyzed solution; The electrolysis process has a first electrolysis process for electrolysis at a constant current and a second electrolysis process for electrolysis at a constant voltage after the first electrolysis process, thereby solving the above-mentioned problem. In the first electrolysis step, a constant current of 1 is applied or two or more constant currents increased stepwise, and in the second electrolysis step, a constant voltage of 1 is applied or two or more constant currents increased stepwise It is preferable to apply a constant voltage. [Selection] Figure 1
priorityDate 2012-08-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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