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filingDate 2019-10-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2022504415-A
titleOfInvention Process for producing isomer-enriched higher silanes
abstract A method for selectively synthesizing n-tetrasilane is disclosed. N-tetrasilane is prepared by thermal decomposition of silane (SiH4), disilane (Si2H6), trisilane (Si3H8) or a mixture thereof. More specifically, the disclosed synthetic methods adjust and optimize the n-tetrasilane: i-tetrasilane isomer ratio. The isomer ratio can be optimized by selecting process parameters such as temperature, residence time and relative amount of starting compound. The disclosed synthetic methods allow easy preparation of n-tetrasilane. [Selection diagram] Fig. 1
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