http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2021024819-A

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D319-06
filingDate 2019-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8123b4c75c2f684bf39a248b86dec1ed
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b4e386e55c3b50e80dc7ca3de1e62d3a
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publicationDate 2021-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2021024819-A
titleOfInvention Method for manufacturing trimethylolpropane cyclic formal
abstract PROBLEM TO BE SOLVED: To provide a manufacturing method for efficiently obtaining CTF. SOLUTION: A step of reacting normal butyraldehyde with formaldehyde in the presence of a basic catalyst to obtain a reaction product solution containing trimethylolpropane (TMP). A step of separating the distillate I containing TMP and the high boiling component from the reaction product solution by distillation. The distillate I is acid-treated and then distilled to separate the distillate II from the high-boiling component containing TMP, and the distillate II is treated by an acetalization reaction and then purified by distillation. A method for producing CTF, which comprises a step of recovering trimethylolpropane cyclic formal (CTF). [Selection diagram] None
priorityDate 2019-08-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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