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publicationDate 2017-08-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2017149901-A
titleOfInvention Method for producing carboxymethylcellulose or a salt thereof, and binder for electrode
abstract When used as a binder for an electrode of a nonaqueous electrolyte secondary battery, carboxymethylcellulose or a salt thereof, which suppresses defects on the electrode surface such as pinholes and has an excellent capacity retention rate of a battery using the same. I will provide a. [MEANS FOR SOLVING PROBLEMS] An alkali celluloseation step (step 1) in which cellulose and alkali are reacted in the presence of a mixed solvent containing water and an organic solvent, and etherification in which the obtained alkali cellulose and etherification agent are reacted. Production of carboxymethylcellulose salt or salt thereof comprising a step (step 2), a purification step (step 3) for washing and drying the obtained reaction mixture, and a pulverization step (step 4) for pulverizing the obtained purified product In the method, step 1 is carried out under conditions of pH 9 or higher and reaction temperature of 5 ° C. or higher and 25 ° C. or lower with a reaction time of 60 minutes or longer and 120 minutes or shorter. [Selection figure] None
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