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filingDate 2014-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2016-10-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2016531152-A
titleOfInvention Method for producing carboxylic acid ester
abstract A process for producing a carboxylic acid ester by reacting a carboxylic acid component with an alcohol component, wherein a liquid carboxylic acid stream is conveyed to the top of a reaction zone maintained under esterification conditions; Transporting the carboxylic acid stream to a countercurrent of the alcohol stream to form a liquid product stream containing the product ester; from the top or near the top of the reaction zone, unreacted alcohol, water, and Removing a purified stream containing ether by-products; flowing the purified stream to a purification zone, treating the stream to reduce its moisture content, and reducing the moisture content below that of the upper stream removed from the reaction zone. Forming an ether-containing stream having; and recycling the ether-containing stream from step (e) to the reaction zone. An apparatus for this method is also described.
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