http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2015020917-A

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filingDate 2013-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2015-02-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2015020917-A
titleOfInvention Process for producing silanes
abstract The present invention provides a method capable of continuously and stably producing an alloy powder containing magnesium silicide on an industrial scale, and a method enabling production of silanes from the alloy powder. A step (I-1) of continuously supplying a raw material mixture containing silicon powder and magnesium powder to a firing furnace under an inert gas atmosphere to continuously raise the temperature of the raw material mixture; The step (I-2) for controlling the temperature of the heated raw material mixture to a specific temperature range, and the alloy powder containing magnesium silicide obtained through the first firing step and the acid are reacted in a solvent. Step (II) for producing silanes, wherein step (I-1) is performed at a temperature rising rate of 2.5 to 50 ° C./min. At a temperature of the raw material mixture containing silicon powder and magnesium powder. It is a step of reaching the first firing temperature in the temperature range of 480 to 520 ° C. (however, the first firing temperature is the temperature range of 480 to 520 ° C. and the heating rate is less than 2.5 ° C./min. The temperature at which the step (I-2) was heated Which is a method for producing silanes, characterized in that to maintain 480-530 for 30 minutes at a temperature range of ° C. (0.5 hours or more. .BACKGROUND
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