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publicationDate 2014-05-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2014091705-A
titleOfInvention Solvent removal method
abstract [PROBLEMS] To remove a solvent used in the production of a sucrose aromatic carboxylic acid ester, which can easily obtain a sucrose aromatic carboxylic acid ester with little coloration and a very small amount of residual solvent. Is to provide a method. A method for removing a solvent used in the production of a sucrose aromatic carboxylic acid ester, wherein a mixture comprising the sucrose aromatic carboxylic acid ester and the solvent is removed by one or more vacuum dryers. , Comprising a series of reduced pressure drying steps in which the pressure and / or heating temperature in the machine is changed under at least two stages and drying under reduced pressure, and the pressure in the first stage of the reduced pressure drying process is lower than atmospheric pressure, And the heating temperature is 20 ° C. or more and 250 ° C. or less, the internal pressure of the final stage of the reduced-pressure drying step is 10 kPa · abs or less, and the heating temperature is 80 ° C. or more and 250 ° C. or less. . [Selection figure] None
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