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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G03G9-08
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B33-18
filingDate 2012-02-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3afc12b17efc25f782b209cd9e406f8b
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publicationDate 2013-08-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2013163622-A
titleOfInvention Method for producing associated silica
abstract Equation (1): Si (OR 1 ) 4 (1) (R 1 is an alkyl group) On the surface of hydrophilic silica composed of SiO 2 units obtained by hydrolyzing and condensing at least one compound selected from the group consisting of tetraalkoxysilanes and partial hydrolysis-condensation products thereof, represented by R 4 Hydrophobicity obtained by hydrophobizing treatment by introducing SiO 3/2 units (R 4 is a monovalent hydrocarbon group) and further introducing R 6 3 SiO 1/2 units (R 6 is a monovalent hydrocarbon group) Hydrophobic silica particles having a carbon content of 2 to 5% by mass, an alkoxy group content of 0.3 to 10% by mass, and an average primary particle size of 0.01 to 200 nm A method for producing associated silica in which two or more primary particles having an average particle diameter in the range of 5 to 500 nm are associated with each other in a humidified atmosphere at a temperature of 100 to 500 ° C. [Effect] Hydrophobized associated silica fine particles obtained by the production method of the present invention are particularly useful as an external toner additive. [Selection figure] None
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