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filingDate 2009-04-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2011-06-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2011517653-A
titleOfInvention Method for producing crystalline material containing lithium, iron and phosphoric acid
abstract The present invention is directed to general formula (I): Li ab M 1 b Fe 1-c M 2 c P de M 3 e O x (I), [Wherein M 1 and M 2 , M 3 , a, b, c, d, e are: M 1 : Na, K, Rb, and / or Cs, M 2 : Mn, Mg, Ca, Ti, Co, Ni, Cr, V, M 3 : Si, S, a: 0.8 to 1.9 b: 0 to 0.3 c: 0 to 0.9, d: 0.8 to 1.9 e: 0 to 0.5, x: 1.0 to 8, (depending on the amount of Li, M 1 Fe, M 2 , P, M 3 and the oxidation state), provided that the compound of the general formula (I) is uncharged. A method for producing a compound represented by: (A) at least one lithium-containing compound, at least one iron-containing compound whose oxidation state of iron is +3, at least one M 1- containing compound if present, and / or at least one M 2 if present. Supplying a mixture comprising a containing compound and / or an M 3 containing compound, if present, and at least one reducing agent that is oxidized to at least one compound having a phosphorus atom with at least one oxidation state of +5; (B) If necessary, the mixture supplied in step (A) is dried to obtain a solid compound, and (C) the solid compound obtained from step (A) or (B) is 300 to 1000 ° C. It is related with the method characterized by including the process baked at the temperature of. [Selection] Figure 2
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