http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2011168485-A

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filingDate 2011-04-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_85b8224704029d7cfae0468f5eea015b
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publicationDate 2011-09-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2011168485-A
titleOfInvention Silica glass containing TiO2 and method for producing the same
abstract A method for producing silica glass containing TiO 2 having a coefficient of thermal expansion of almost zero over a wide temperature range is provided. A method for producing silica glass containing TiO 2 , comprising: (a) depositing silica glass fine particles obtained by flame hydrolysis of a Si precursor and a Ti precursor, which are glass forming raw materials, on a substrate; A step of growing to form a porous glass body; (b) a step of heating the porous glass body to a transparent vitrification temperature to obtain a transparent glass body; and (c) a transparent glass body at a softening point or higher. A step of obtaining a molded glass body by heating to a temperature of 5 ° C., and (d) holding the molded glass body at a temperature exceeding 500 ° C. for 5 hours or more and then up to 500 ° C. at 10 ° C./hr or less. An annealing process for lowering the temperature at an average temperature lowering rate. [Selection] Figure 1
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