http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2008291008-A

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D295-125
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C51-60
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C57-32
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C51-00
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D295-18
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filingDate 2008-04-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_302a322ecf1f890d3e4710c19118f5b9
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_45d023c6dcc90beb8d6f001e14e1a152
publicationDate 2008-12-04-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2008291008-A
titleOfInvention 2,5-dimethylacetophenone derivative, 2,5-dimethylphenylacetic acid obtained from 2,5-dimethylacetophenone derivative and method for producing the same
abstract The present invention provides a high-purity 2.5-dimethylacetophenone derivative, 2,5-dimethylphenylacetic acid obtained from a 2.5-dimethylacetophenone derivative and a derivative thereof in a high yield. 2,5-dimethylacetophenone, sulfur, and morpholine are reacted at a temperature of 100 ° C. or higher and lower than the boiling point of the reaction system to produce 2,5-dimethylphenylthioacetomorpholine. The temperature may be about 100 to 125 ° C. The manufacturing method may include a step of isolating 2,5-dimethylphenylthioacetomorpholine by crystallization. Moreover, in the said manufacturing method, the ratio of sulfur may be about 1-2 mol with respect to 1 mol of 2, 5- dimethyl acetophenone, and the ratio of morpholine may be excess mol. [Selection figure] None
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