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filingDate 2003-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2005-11-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2005535759-A
titleOfInvention Siloxane bischloroformate
abstract Siloxane bischloroformate is prepared in a continuous process by phosgenating siloxane bisphenol with a substantial excess of phosgene and sodium hydroxide in a flow reactor. A very high level (> 95%) conversion of siloxane bisphenol to the corresponding siloxane bischloroformate is achieved using a flow reactor according to the process of the present invention, whereas using a similar batch process, Conversion of siloxane bisphenol to the corresponding siloxane bischloroformate can only be achieved with a lower conversion (about 90%). The method of the present invention can be expected to be used in the production of silicone-containing copolycarbonates that require high purity siloxane bischloroformate intermediates.
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