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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-6574
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filingDate 2004-01-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d7f943934d10e31d143d1ea95758173c
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publicationDate 2005-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2005200325-A
titleOfInvention Method for producing phosphite crystals
abstract PROBLEM TO BE SOLVED: To produce crystals of (I) at a high recovery rate when crystallizing two batches or more of the following phosphites (I) continuously in a batch system. The following first to sixth steps are included. First step: Cooling and crystallizing a liquid containing the above-mentioned (I) and the crystallization solvent in the first batch in a batch system. Second step: A slurry containing the produced (I) and the crystallization solvent is filtered to obtain a crude wet cake. Third step: The crude wet cake is washed with a washing solvent to obtain a fine wet cake and a first batch of washing liquid. Fourth step: Cooling and crystallizing the liquid containing the (I) of the second batch, the crystallization solvent, and the washing liquid of the first batch in a batch system. Fifth step: The slurry containing the produced (I), the crystallization solvent and the first batch of washing liquid is filtered to obtain a crude wet cake. Step 6: After washing the rough wet cake with a washing solvent, a step of obtaining a fine wet cake and a second batch of washing liquid [Selection figure] None
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2012513404-A
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