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filingDate 2000-12-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e3cf22343244c5cc15935257c005e7c1
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publicationDate 2002-07-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-2002187709-A
titleOfInvention Manufacturing method of graphite powder
abstract (57) [Summary] [Problem] A lithium ion having a discharge capacity of 350 mAh / g or more, which is close to the theoretical capacity, a charge / discharge efficiency of as high as 90% or more, and a charge / discharge efficiency that is unlikely to be reduced even in large current discharge or low temperature discharge A graphite powder suitable for a negative electrode material of a secondary battery is stably manufactured. SOLUTION: Tar and / or pitch having a free carbon content of 0.1% by mass or less and a toluene-insoluble content of 5% by mass or less purified by a ketone solvent are preferably heated to 250 to 400 ° C. in the presence of a nitrating agent. After heating and polycondensation treatment, the bulk mesophase carbon obtained by heat treatment in the temperature range of 400 to 600 ° C is pulverized by one or both of high-speed impact pulverization at 5000 rpm or more and shear pulverization, and carbonized and graphitized. Manufacture graphite powder. This graphite powder has a d00 2 is less than 3.360 mm and has high crystallinity with a crystallite thickness of 350 mm or more.
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